By J. F. Coetzee, D. Frollini (auth.), Gleb Mamantov (eds.)
This ebook includes contributions by way of contributors within the Symposium "Spectroscopic and Electrochemical Characterizat.ion of Solute Species in Non~Aqueous Solvents" which happened on the American Chemical Society assembly, department of Analytical Chemistry, August 31 and September I, 1976, San Francisco, California. The manuscripts have been submitted to the editor in the course of the first 1/2 1977 and, mostly, symbolize studies of chosen study issues within the extensive quarter of characterization of solute species in non~aqueous solvents. In organizing this Symposium, i tried to compile a considerably huge crew of analysis employees considering spectro scopic and electrochemical reviews within the 3 huge periods of non-aqueous solvents ~ natural solvents, covalent inorganic sol vents and molten salts. The experimental apprcaches and difficulties, resembling avoidance of lines of moisture and oxygen, are often related for all sorts of non-aqueous solvents. it's was hoping that this quantity might be valuable to all eager about chemistry in non-aqueous solvents. Gleb l>lamantov , Contents 1. identity AND SYSTEMIZATION OF SOLVENT houses concerned about THE LIGAND SUBSTITUTION KINETICS OF LABILE COMPLEXES OF NICKEL(II) J. F. Coetzee, D. Frollini, C. G. Karakatsanis, E. J.
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Dalton, 1602 (1973). F. COETZEE ET AL. (56) H. P. Bennetto and E. F. Caldin, J. Chern. Soc. A, 2191, 2198, 2207 (1971); H. P. Bennetto, ibid~, 2211 (1971)~ (57) J. A. Riddick and W. B. Bunger, "Organic Solvents," WileyInterscience, New York (1970). (58) T. B. Reddy, Pure ~. , (59) J. Juillard, Pure ~. , in press. (60) J. F. Coetzee, Pure Appl. Chern. , ~, 427 (1966) . (61) J. F. Coet zee, Pure Appl. Chern. , in press. (62) J. F. Coetzee and K. Umemoto, Inorg. Chern. , (63) T. Fuj inaga and K.
55 390 (1967) . ALKALI METAL, MAGNESIUM-25, AND SILVER-lOg NMR STUDIES OF COMPLEX COMPOUNDS IN NONAQUEOUS SOLVENTS Alexander I. Popov Department of Chemistry, Michigan State University East Lansing, Michigan 48824 INTRODUCTION At the present time we have at our disposal a large variety of experimental techniques for the characterization of solute species in solutions and the studies of their properties. Among these nuclear magnetic resonance of metallic nuclei is becoming an increasingly important probe of their behavior in solutions and, in particular, of very weak interactions of the respective ions with solvents, counterions, or complexing agents.
Phys. Chem. , 67, 1810 (1963) . (5) V. Gutman, "Coordination Chemistry in Nonaqueous Solutions," Springer-Verlag, New York, New York, 1968, p. 19. (6) M. R. Olds and R. T. Iwamoto, Anal. , 47, 2394 (1975). , ~, 55 390 (1967) . ALKALI METAL, MAGNESIUM-25, AND SILVER-lOg NMR STUDIES OF COMPLEX COMPOUNDS IN NONAQUEOUS SOLVENTS Alexander I. Popov Department of Chemistry, Michigan State University East Lansing, Michigan 48824 INTRODUCTION At the present time we have at our disposal a large variety of experimental techniques for the characterization of solute species in solutions and the studies of their properties.